Different microreactor systems are available at our research group:
Labtrix® Start (Chemtrix) Internal volume: 1, 5 or 10 µl depending on the reactor chip used Temperature range: -15°C to 195°C Pressures up to 25 bar Wetted materials: glass, PEEK, PTFE, Techtron
KiloFlow® (Chemtrix) Internal volume: 13 ml Temperature range: 10°C to 150°C Pressures up to 20 bar Wetted materials: glass, PEEK, ETFE, perfluoroelastomer
X-CubeTM (ThalesNano) Temperature range: 20°C to 200°C Pressures up to 150 bar Wetted material: stainless steel Compatible with gases (H2, O2, ...) Compatible with catalyst cartridges (Pd/C, Raney Ni, ...)
Uniqsis FlowSyn Flow rates from 5 µl/min up to 10 ml/min Glass static mixer + Teflon 5 ml coil reactor 10 bar BPR
In house assembled microreactor PEEK T- or Y-mixer or ETFE T-mixer PFA-tubing (0.5 mm internal diameter)
CPC® College System 2 ml microreactor (stainless steel) + 45 ml residence time unit
Bruker Avance-III 400 MHz NMR Spectrometer equipped with BRUKER 5 mm BBFO 400 MHz Z-gradient high resolution probe
Description
State-of-the-art NMR spectrometer equipped with an observe broadband high resolution probe, fitted with an actively shielded single axis Z-gradient for 5 mm sample diameters and 400 MHz standard-bore or wide-bore magnets. The inner NMR coil can be tuned to observe 19F or any nucleus in the range from 31P to 15N. The outer NMR coil is tuned for either 1H decoupling or observation. The probe is fitted with a 2H lock channel and automatic tuning and matching (ATM).
Signal/Noise
19F sensitivity ≥250:1 (TFT sample, with 1H decoupling)
